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Breathing Gas Analyser: Protea Model BG100

For Fighter Pilots * Professional Divers * Fire Fighters * Hospital Patients

BG 100

Protea's Breathing Gases Analyser System detects and measures impurities in the bottled breathing gases used by pilots, divers, fire-fighters and hospital patients. It meets current standards such as USAF MIL-O-27210, NATO STANAG 3545 and MoD 68-284.

System SoftwarePowerful analyser control and analysis software is used. A convenient sampling system is also supplied which regulates the flow of sample gas to the analyser, allows easy change-over between samples, and maximises analysis accuracy. Analysis results are presented to the user in standard and customised report formats within a few minutes and all collected spectra and reports are stored with a unique date/time/sample identification stamp.

The system uses an ABB Bomem Inc FTIR analyser. To calibrate additional gases, a convenient septum interface is provided on the sample cell for injecting measured amounts of reference gases.



FEATURES AND BENEFITS OF THE BG100:

Features User Benefits
FTIR-based analyser The high resolution of FTIR and its inherent stability over extended periods allows simultaneous analysis of many species, with minimal interference.
Accuracy The system has been extensively calibrated for a range of components using traceable reference standards.
Sensitivity The system uses a MCT detector and multi-pass long path-length gas cell. These combine to give detection limits for some of the calibrated gases down to single ppb levels.
Flexibility Many components can be detected simultaneously. The standard system comes calibrated for 11 components, although more can be accommodated.
Fast response time Sample turn-around time is typically 6 per hour, including cylinder handling.
Automated operation The BG100 can be used by minimally-skilled operators

THE SAMPLING SYSTEM

Sampling SustemThe sampling methodology used with the BG100 is shown in the opposite figure. The sampling system is used to prepare the sampling cell on the FTIR analyser for a reference by purging with dry nitrogen. It is also used to purge the gas cell with sample. To verify system performance, or to perform additional calibrations, the sampling system can also prepare the cell for a gas or volatile liquid injection. The cell is first purged with nitrogen, then partially evacuated just prior to the injection. After the sample is injected into the gas cell using a septum connection, the sampling system restores the gas cell pressure using nitrogen. Due to the low concentrations required for the determination of trace gases, the use of syringes to inject small volumes of a gas or liquid proves very convenient.

THE SOFTWARE

Client ReportProtea has developed a user interface and custom report forms specific for the Breathing Gases application which operate within Grams. Grams is a powerful tool which allows the user to perform spectral analysis. Protea's user interface simplifies and automates the use of Grams - to control the FTIR analyser, to operate the sampling system, to analyse and save spectra, and to prepare customised reports. Operation of these through the user interface is quite simple. However, the user has access to the full power of Grams if needed.

Note: Grams LT is supplied as standard, and is a product of Thermo Electron Corporation

SPECIFICATIONS

Sampling SystemThe following specifications apply for the analysis of breathing oxygen for fighter pilots in accordance with Military Standard MIL-O-27210. The gas components measured are given in the table below, together with their Limit Of Detection (LOD) and procurement limits as required by the Standard. For maximum accuracy, Protea has calibrated each of the 11 components over an 11-point range up to the procurement limit. An advanced mathematical calibration model based on partial least squares (PLS) has been compiled using all such data points. The concentrations of Freon 12, 22, and 113 are reported separately in the standard report, as are solvents 1,1,1 Trichloroethane and Trichloroethylene. The measurement time is less than 2 minutes using an MCT detector. The concentration precision is generally better than ±10% in the calibrated range for each component. This includes the effects of interference by other components. The analyser can be calibrated for a wide variety of additional trace contaminants in breathing air. It can also be used for other gas analysis applications.

Gases Measured for Military Standard MIL-O-27210

Component Sub-component Procurement Limit *
(Type 1 Oxygen), ppm
Calibration
Range ppm
LOD
ppb
CO2 carbon dioxide 10 0 - 10 282
CH4 Methane 50 0 - 50 130
C2H2 Acetylene 0.1 0 - 0.1 2
C2H4 Ethylene 0.4 0 - 0.4 9
C2H6 Ethane 6 0 - 6 10
N2O nitrous oxide 4 0 - 4 28
Freons Freon 12, Freon 22, Freon 113 2.0 0 - 2.0 68
Solvents 1,1,1- trichloroethane, trichloroethylene 0.2 0 - 0.2 6
 
       
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